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- W2100331337 abstract "The interaction of oxygen/hydrogen gas mixtures with Rh crystals was studied by means of video-FIM (field ion microscopy) at temperatures between 400 and 500 K and total pressures up to 10 -2 Pa. Rh samples were found to suffer considerable morphological changes during the reaction at 505 K and relative gas amounts of H 2 /O 2 = 0.1…9. Strong faceting of planes lying along the zone lines was seen and interpreted as being oxygen-driven. The surface structures changed while removing hydrogen from the gas mixture. In situ video-FIM allowed us to monitor the time dependence of changes. Accordingly, planes lying along the zone lines transformed first from O ad /H ad into O ad -covered The process started in {011 } planes and finally reached the (001) pole. A cross-like image feature thus appeared and divided the apex surface of the Rh crystal into four equivalent quadrants with {111 } planes in their center. These quadrants reacted subsequently in an independent manner, that is, the transformation from an O ad /H ad mixed layer into an O ad layer occurred with a delay period of up to several minutes while decreasing the hydrogen gas pressure. The structural changes observed were reversible upon increasing the hydrogen gas pressure." @default.
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- W2100331337 date "2000-05-01" @default.
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- W2100331337 title "Field ion microscopy study of the structural changes in Rh crystals during the reaction of oxygen–hydrogen gas mixtures" @default.
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- W2100331337 doi "https://doi.org/10.1016/s0039-6028(00)00233-8" @default.
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