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• W2100363003 abstract "Migration behavior and enantioseparation of racemic hydrobenzoin and structurally related compounds, including benzoin and benzoin methyl ether, in CZE with a dual CD system consisting of heptakis-(2,3-dihydroxy-6-O-sulfo)-β-CD (SI-S-β-CD) and β-CD as chiral selectors in the presence and absence of borate complexation at pH 9.0 were investigated. The results indicate that enantioseparation of hydrobenzoin is mainly governed by CD complexation of hydrobenzoin–borate complexes with SI-S-β-CD when SI-S-β-CD concentration is relatively high. Whereas CD complexation of hydrobenzoin–borate complexes with β-CD plays a significant role in enantioseparation when SI-S-β-CD concentration is comparatively low. The (S,S)-enantiomer of the hydrobenzoin–borate complex was found to interact more strongly than the corresponding (R,R)-enantiomer with both SI-S-β-CD and β-CD. These two types of CD show the same chiral recognition pattern, but they exhibit opposite effects on the mobility of the enantiomers of hydrobenzoin–borate complexes. Enantiomer migration reversal of hydrobenzoin occurred in the presence of borate complexation when varying the concentration of β-CD, while keeping SI-S-β-CD at a relatively low concentration. Binding constants of the enantiomers of benzoin-related compounds to β-CD and those of hydrobenzoin–borate complexes to SI-β-CD were evaluated; the mobility contributions of all complex species to the effective mobility of the enantiomers of hydrobenzoin as a function of β-CD concentration in a borate buffer were analyzed. In addition, comparative studies on the enantioseparation of benzoin-related compounds with SI-S-β-CD and with randomly sulfate-substituted β-CD were made." @default.
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• W2100363003 date "2005-11-01" @default.
• W2100363003 modified "2023-10-16" @default.
• W2100363003 title "Migration behavior and enantioseparation of hydrobenzoin and structurally related compounds in capillary zone electrophoresis with a dual cyclodextrin system consisting of heptakis-(2,3-dihydroxy-6-O-sulfo)-β-cyclodextrin and β-cyclodextrin" @default.
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• W2100363003 doi "https://doi.org/10.1002/elps.200500294" @default.
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