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- W2100537207 abstract "A thermophysical study of the sulfur containing amino acids l-cysteine and l-cystine has been carried out by differential scanning calorimetry (DSC). Heat capacities of both compounds were measured in the temperature interval from T = 268 K to near their respective melting temperatures. DSC and variable temperature powder X-ray diffraction analysis (PXRD) gave evidence for a solid–solid phase transition close to the melting point only in the l-cysteine sample. DSC experiments show that this solid–solid transition is not reversible in the temperature interval T = 235–485 K and presents a behavior depending on heating temperature, time, and rate. This behavior is also supported by variable-temperature PXRD. The patterns for the commercial samples, at room temperature, are consistent with those simulated for the orthorhombic and hexagonal polymorphic forms from the single-crystal X-ray analysis." @default.
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- W2100537207 date "2011-02-27" @default.
- W2100537207 modified "2023-09-27" @default.
- W2100537207 title "Thermal behavior and polymorphism in medium–high temperature range of the sulfur containing amino acids l-cysteine and l-cystine" @default.
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- W2100537207 doi "https://doi.org/10.1007/s10973-011-1302-6" @default.
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