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- W2100672560 endingPage "4188" @default.
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- W2100672560 abstract "The gelation mechanism and cross-link inhomogeneity of phenolic resins prepared via polycondensation of phenol and formaldehyde under acidic conditions were studied by using 13C-NMR spectroscopy and small-angle X-ray scattering. The structural analysis of the gelation process indicated the presence of two different mechanisms of the formation and growth of the inhomogeneity that depend on the initial formaldehyde-to-phenol molar ratio: (i) when there is an insufficient amount of a cross-linker at the initial stage of gelation, inhomogeneous domains with a loosely cross-linked network appear and the degree of cross-linking in the domain increases with the reaction time. (ii) When there is a sufficient amount of a cross-linker at the initial stage of gelation, inhomogeneous domains with a tightly cross-linked network appear, followed by an increase in the size of the domains." @default.
- W2100672560 created "2016-06-24" @default.
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- W2100672560 date "2013-01-01" @default.
- W2100672560 modified "2023-10-01" @default.
- W2100672560 title "Gelation and cross-link inhomogeneity of phenolic resins studied by 13C-NMR spectroscopy and small-angle X-ray scattering" @default.
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- W2100672560 doi "https://doi.org/10.1039/c3sm27438a" @default.
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