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- W2100687599 abstract "A series of novel Shiff bases (1a–h) was synthesized by condensation of pyridinecarboxaldehydes (1–4) with 3- and 4-trifluoromethylanilines (5, 6) in the presence of molecular sieves (4 Å). It was found that AlCl3 and AlBr3 catalyzed the addition of Me3SiCN to the CN bond of the imines obtained, whereas the other Lewis acids studied (YCl3, LaCl3, ZnI2) were not active. The reactivity of the imines in the title reaction, on the whole, correlated with their basicity. Besides the addition giving the expected α-amino nitriles (2a,b,d–f,h), an unusual reaction leading to unsaturated nitriles (3a–h) was observed. The structures of saturated and unsaturated products 2d and 3c were determined by X-ray diffraction. Copyright © 2001 John Wiley & Sons, Ltd." @default.
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- W2100687599 date "2001-01-01" @default.
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- W2100687599 title "Addition of Me3SiCN to trifluoromethyl derivates ofN-(pyridylmethylidene) anilines catalyzed by Lewis acids" @default.
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- W2100687599 doi "https://doi.org/10.1002/aoc.223" @default.
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