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- W2100695556 abstract "Photolysis of Re( i PrCp)(CO) 2 (PF 3 ) in liquid or supercritical Xe yields two new compounds [Re( i PrCp)(CO) 2 Xe and Re( i PrCp)(CO)(PF 3 )Xe]. Re( i PrCp)(CO)(PF 3 )Xe has been characterized by NMR and IR spectroscopies. The compound is an organometallic Xe complex that has been characterized by using NMR spectroscopy and is shown to be longer-lived than other organometallic Xe complexes by IR spectroscopy. 19 F, 31 P, and 129 Xe chemical shifts have been determined. The 129 Xe chemical shift of Re( i PrCp)(CO)(PF 3 )Xe, δ –6,179, is a Xe shift that is significantly shielded, on the order of 1,000 ppm, with respect to free Xe. The coupling constants between coordinated 129 Xe and both the 19 F and 31 P nuclei present have been extracted, confirming the identity of the compound. Observed line widths give a lower limit to the lifetime of the coordinated Xe of 27 ms at 163 K." @default.
- W2100695556 created "2016-06-24" @default.
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- W2100695556 date "2005-01-27" @default.
- W2100695556 modified "2023-10-18" @default.
- W2100695556 title "Characterization of an organometallic xenon complex using NMR and IR spectroscopy" @default.
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- W2100695556 doi "https://doi.org/10.1073/pnas.0406527102" @default.
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