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- W2100947853 abstract "Abstract Combination of coordination polymerization and atom transfer radical polymerization (ATRP) was applied to a novel synthesis of rod‐coil block copolymers. The procedure included the following steps: (1) monoesterification reaction of ethylene glycol with 2‐bromoisobutyryl bromide yielded a α‐bromo, ω‐hydroxy bifunctional initiator, (2) CpTiCl 3 (bifunctional initiator) catalyst was prepared from a mixture of trichlorocyclopentadienyl titanium (CpTiCl 3 ) and bifunctional initiator. Coordination polymerization of n‐ butyl isocyanate initiated by such catalyst provided a well‐defined macroinitiator, poly( n‐ butyl isocyanate)‐Br (PBIC‐Br), and (3) ATRP method of vinyl monomers using PBIC‐Br provided rod (PBIC)‐coil block copolymers. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 4037–4042, 2007" @default.
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- W2100947853 date "2007-07-17" @default.
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- W2100947853 title "Novel synthesis of rod-coil block copolymers by combination of coordination polymerization and ATRP" @default.
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- W2100947853 doi "https://doi.org/10.1002/pola.22157" @default.
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