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- W2101612842 abstract "Abstract Bis(hexafluoroisopropyl) fumarate (BHFIPF) did not homopolymerize with free radical initiators. However, BHFIPF yielded alternating copolymers with styrene in bulk with Azobisisobutyronitrile (AIBN) as a radical initiator. The monomer reactivity ratios of BHFIPF ( M 1 ) and styrene ( M 2 ) were calculated as r 1 = 0.00 and r 2 = 0.02. BHFIPF also copolymerized with vinyl pentafluorobenzoate (VPFB) in bulk and in pentafluoroisopropanol solution to produce an alternating copolymer. The reactivity ratios of BHFIPF ( M 1 ) with VPFB ( M 2 ) were r 1 = 0.00 and r 2 = 0.05 in bulk and r 1 = 0.01 and r 2 = 0.11 in pentafluoroisopropanol, respectively. The glass transition temperatures ( T g ) of the BHFIPF‐styrene and BHFIPF‐VPFB copolymers were 107 and 86 °C, respectively. The BHFIPF‐styrene copolymer was thermally stable, and the thermal degradation temperature ( T d ) was 400 °C, whereas the T d of BHFIPF‐VPFB copolymer was 240 °C. The films obtained by casting from tetrahydrofuran (THF) solutions of these copolymers were flexible and transparent. Their refractive indices were 1.4048 for the BHFIPF‐styrene copolymer, and 1.3980 for the BHFIPF‐VPFB copolymer at 633 nm, respectively. © 2011 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem, 2011" @default.
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- W2101612842 date "2011-05-04" @default.
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- W2101612842 title "Alternating copolymerization of bis(hexafluoroisopropyl) fumarate with styrene and vinyl pentafluorobenzoate: Transparent and low refractive index polymers" @default.
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- W2101612842 doi "https://doi.org/10.1002/pola.24717" @default.
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