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• W2101669898 abstract "The bulky m-terphenyl phenol Ar*OH 1 (Ar* = C 6 H 3 -2,6-Mes 2 , Mes = 2,4,6-trimethylphenyl) was synthesized via the treatment of Ar*Li with nitrobenzene. The phenol 1 is prepared in modest to good yield using this method. Attempts were also made to prepare 1 through oxidation of the bulky boronic acid Ar*B(OH) 2 with Oxone ® , but this reaction was not suitable for preparative-scale reactions. Side products of the reaction between Ar*Li and nitrobenzene were identified as Ar*[N(O)Ph] and [C 6 H 5 N(O)] 2 and were characterized by X-ray crystallography and EPR spectroscopy. A variety of main-group and transition-metal complexes of Ar*OH were prepared, namely Sn(OAr*) 2 , Ge(OAr*) 2 , [N(SiMe 3 ) 2 ]Ge(OAr*), [Me 2 Al(OAr*)] 2 , and Ti(NMe 2 )(OAr*) 2 . All compounds were characterized spectroscopically and most were studied by single-crystal X-ray diffraction as well.Key words: m-terphenyl, main-group compounds, X-ray crystallography, multinuclear NMR spectroscopy, EPR spectroscopy." @default.
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• W2101669898 date "2008-01-01" @default.
• W2101669898 modified "2023-09-27" @default.
• W2101669898 title "Synthesis of the bulky<i>m</i>-terphenyl phenol Ar*OH (Ar* = C₆H₃-2,6-Mes₂, Mes = 2,4,6-trimethylphenyl) and the preparation and structural characterization of several of its metal complexes" @default.
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• W2101669898 doi "https://doi.org/10.1139/v07-131" @default.
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