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- W2103178043 abstract "The crystallisation of the nucleation agent ZrTiO4 in a low thermal-expansion lithium aluminosilicate glass-ceramics is monitored as a function of time by combining transmission electron microscopy with Ti-L2,3 X-ray absorption near-edge structure spectroscopy. The formation of liquid–liquid phase-separation droplets is shown to precede ZrTiO4 crystallisation within the latter nanosized droplets. Quantitative data on crystalline fractions enable conclusions on the self-limited growth of ZrTiO4 nanocrystals in low thermal-expansion glass-ceramics and based on Avrami's equation, the growth is shown to be restricted by a barrier (the outer border of the phase-separation droplet). It is shown that liquid–liquid phase separation and crystallisation are temporally decoupled. The size of ZrTiO4 crystallites is determined by the restricted volume of the phase-separation droplets they crystallise in. The volume of the droplets in turn is restricted by the formation of a diffusion barrier in the surrounding residual glass." @default.
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- W2103178043 date "2011-01-01" @default.
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- W2103178043 title "ZrTiO4 crystallisation in nanosized liquid–liquid phase-separation droplets in glass—a quantitative XANES study" @default.
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- W2103178043 doi "https://doi.org/10.1039/c0ce00716a" @default.
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