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• W2103240158 endingPage "428" @default.
• W2103240158 startingPage "420" @default.
• W2103240158 abstract "Abstract Four novel organotin complexes of two types—[R 2 Sn( o ‐SC 6 H 4 CO 2 )] 6 (R=Me, 1 ⋅H 2 O; n Bu, 2 ) and {[R 2 Sn( m ‐CO 2 C 6 H 4 S)R 2 Sn( m ‐SC 6 H 4 CO 2 )SnR 2 ]O} 2 (R=Me, 3 ; n Bu, 4 )—have been prepared by treatment of o ‐ or m ‐mercaptobenzoic acid and the corresponding R 2 SnCl 2 (R=Me, n Bu) with sodium ethoxide in ethanol (95 %). All the complexes were characterized by elemental analysis, FT‐IR and NMR ( 1 H, 13 C, 119 Sn) spectroscopy, TGA, and X‐ray crystallography diffraction analysis. The molecular structure analyses reveal that both 1 and 2 are hexanuclear macrocycles with hydrophobic “pseudo‐cage” structures, while 3 and 4 are hexanuclear macrocycles with double‐cavity structures. Furthermore, the supramolecular structure analyses show that looser and more intriguing supramolecular infrastructures were also found in complexes 1 – 4 , which exist either as one‐dimensional chains of rings or as two‐dimensional networks assembled from the organometallic subunits through intermolecular CH⋅⋅⋅S weak hydrogen bonds (WHBs) and π–π interactions." @default.
• W2103240158 created "2016-06-24" @default.
• W2103240158 creator A5000546219 @default.
• W2103240158 creator A5032199627 @default.
• W2103240158 creator A5061485530 @default.
• W2103240158 creator A5061492989 @default.
• W2103240158 date "2005-12-19" @default.
• W2103240158 modified "2023-10-17" @default.
• W2103240158 title "Self-Assembly of Dialkyltin Moieties and Mercaptobenzoic Acid into Macrocyclic Complexes with Hydrophobic “Pseudo-Cage” or Double-Cavity Structures: Supramolecular Infrastructures Involving Intermolecular CH⋅⋅⋅S Weak Hydrogen Bonds and π–π Interactions" @default.
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