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- W2103335528 abstract "A series of cationic and dicationic Ru-arene complexes with Binap (1a) and MeO-Biphep (1b) have been prepared. 13 C NMR studies are shown to be useful in connection with recognising the 6e-bonding mode of 1a and 1b in the dications [Ru(1a or 1b)(η 6 -arene)](SbF 6 ) 2 (8,9). Reaction of 8,9 with: (a) (Bu 4 N)(Ph 3 SiF 2 ) leads to a cyclometallated product which arises via PC bond breaking and PF bond making; (b) methanol provides a straightforward synthesis of the corresponding hydrides. 13 C NMR p-cymene chemical shifts are reported.Key words: PC bond cleavage, 6e donors, cyclometallation, hydrides, 13 C NMR." @default.
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- W2103335528 date "2001-05-01" @default.
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- W2103335528 title "Binap and MeO-Biphep complexes of Ru(II). Dicationic ligands as 6e donors. Unexpected cyclometallation in connection with PC bond breaking" @default.
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- W2103335528 doi "https://doi.org/10.1139/v00-156" @default.
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