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- W2103403211 abstract "Abstract A novel route to functionalized azulenes is devised from a dihydroazulene precursor. Thus, bromination of 1,1‐dicyano‐2‐phenyl‐1,8a‐dihydroazulene followed by heating in the presence of bromide ions provides an efficient way to generate 3‐bromo‐1‐cyano‐2‐phenylazulene. Formation of this somewhat unexpected product was confirmed by X‐ray crystallographic analysis. It undergoes a palladium‐catalyzed cross‐coupling reaction with trimethylsilylacetylene, affording a new azulene building block for acetylenic scaffolding. Oxidative homo‐coupling hereof provides an azulene dimer, for which the optical and electrochemical properties are compared to the other azulenes. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)" @default.
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- W2103403211 date "2007-03-01" @default.
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- W2103403211 title "A Novel Route to a Bromo‐Cyano‐Substituted Azulene and Its Exploitation in the Construction of an Acetylenic Scaffold" @default.
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- W2103403211 doi "https://doi.org/10.1002/ejoc.200601052" @default.
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