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- W2103754189 abstract "The crystal structures of trans,trans-Ethyl-5-(4-chlorophenylsulfonyl)-4-hydroxy-2,6-dip-tolyl-1,2,5,6-tetrahydropyridine-3-carboxylate (Ia) and cis-Diethyl 4-hydroxy-2-(4-nitrophenyl)-5-(phenylsulfonyl)-6-(phenylsulfonylmethyl)cyclohexa-3,6-diene-1,3-dicarboxylate (Ib) were elucidated by single crystal X ray diffraction. Compound (Ia) C 28 H 28 Cl NO 5 S, crystallizes in the monoclinic system, space group P 2 1 /c, with a = 9.4530(7) A, b = 25.366(2) A, c = 11.4353(8) A, β = 103.092(7)°, V = 2670 (3) A 3 and Z = 4. The compound (Ib), C 31 H 29 N 1 O 11 S 2 , crystallizes in the monoclinic system, space group P 2 1 /c, with a = 21.179(4) A, b = 8.4998(16) A, c = 17.347(3) A, β = 102.563(3)°, V = 3048.0(10) A 3 and Z = 4. The central piperidine ring of compound (Ia) adopts the sofa conformation and the central cyclohexadiene ring of compound (Ib) adopts the boat conformation. Details of the compounds preparation, crystal structures and hydrogen bonding interactions of the compounds are discussed." @default.
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- W2103754189 date "2012-10-18" @default.
- W2103754189 modified "2023-09-24" @default.
- W2103754189 title "Crystal structural studies of ethyl-5-(4-chlorophenylsulfonyl)-4-hydroxy-2, 6-dip-tolyl-1, 2, 5, 6-tetrahydropyridine-3-carboxylate and diethyl 4-hydroxy-2-(4-nitrophenyl)-5-(phenylsulfonyl)-6-(phenylsulfonylmethyl)cyclohexa-3,6-diene-1,3-dicarboxylate" @default.
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