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- W2104348506 abstract "From the study of the hypothetical series Pb[PbInc–2pSbc]O6+p (O ⪕ p < 1; 0 ⪕ c < 2), the existence of the cubic pyrochlore Pb2II[In0.5Sb1.5]O6.5 has been established. This compound was obtained as an orange yellow powder, S.G. Fd4m (No. 227), Z = 8, a = 10.5892(1) Å, V = 1187.38(3) Å3, Dc = 8.48 M gm−3. For Pb in 16(c) positions, In and Sb (1:3) randomly distributed in 16(d), oxygen atoms in 48(f) and in a half of the 8(a) sites, and oxygen positional parameter x = 0.429 (origin at center, 3m), R = 0.062. The apparent interatomic distances (Å) are determined: PbO = 2.612; (In, Sb)O = 2.019. Das neue Pyrochlor Pb [In0,5 Sb1,5]O6,5. Bei Untersuchungen in der hypothetischen Serie Pb[PbInc–2pSbc]O6+p(0 ⪕ p < 1; 0 ⪕ c < 2) wurde ein neues Oxid von gelboranger Farbe gefunden, Zusammensetzung Pb[In0,5Sb1,5]O6,5, mit einer Pyrochlorstruktur (R.G. Fd3m), Z = 8, a = 10,5892(1) Å, Dc = 8,48 M gm−3. Der Vergleich der beobachteten und berechneten Intensitäten im Röntgenpulver-Diffraktegramm ergab Pb in 16(c), statistische Verteilung von In und Sb (1:3) in 16(d), Sauerstoffatome in 48(f) und der Hälfte der 8(a) Positionen, und Sauerstofflageparameter von x = 0,429 (Koordinatenursprung im Inversionszentrum, 3m), mit einem R-Wert von 6,2%. Die beobachteten Abstände (Å) betragen PbO = 2,612, (In, Sb)O = 2,019." @default.
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- W2104348506 date "1985-10-01" @default.
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- W2104348506 title "New Pyrochlore Pb2II[In0.5 Sb1.5]O6.5" @default.
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- W2104348506 doi "https://doi.org/10.1002/zaac.19855291029" @default.
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