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- W2104395021 abstract "A new method for the preparation of indoles from readily available alpha-haloenones and alpha-(trialkylstannyl)enecarbamates is described. Following a Stille coupling, trienecarbamate 2 is electronically activated to undergo a facile 6pi-electrocyclic ring closure and subsequent oxidation to afford protected aniline 4. Upon deprotection and reductive amination, acid 5 underwent clean cyclization to N-acetylindole 6 (Ac2O, NEt3, 130 degrees C). This method has been used to construct a variety of substituted indoles that are not easily prepared by conventional indole annelation methods." @default.
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- W2104395021 date "2006-03-30" @default.
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- W2104395021 title "Synthesis of Indoles via 6π-Electrocyclic Ring Closures of Trienecarbamates" @default.
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- W2104395021 doi "https://doi.org/10.1021/ja060282o" @default.
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