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- W2104826518 abstract "Die Gemische der stereoisomeren 2,3-, 2,4- und 3, 4-Dimethylpiperidine warden durch katalytische Hydrierung der entsprechenden Lutidine dargestellt. Die einzelnen Isomeren warden durch fraktionierte Destillation getrennt. Die Konfigurationsaufklärung erfolgt kernresonanzspektroskopisch durch Analyse der 100 und 220 MHz NMR Spektren. Es gelingt eine weitgehende Zuordnung aller Protonen des Piperidinringes. Mixtures of the stereoisomeric 2,3-, 2,4- and 3,4-dimethylpiperidines have been prepared by catalytic hydrogenation of the corresponding lutidines and the isomers have been separated by fractional distillation. Configurational assignments are made on the basis of the corresponding 100 and 220 MHz NMR spectra. In most cases an almost complete assignment of all protons, in the piperidine ring, was possible." @default.
- W2104826518 created "2016-06-24" @default.
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- W2104826518 date "1969-02-01" @default.
- W2104826518 modified "2023-10-16" @default.
- W2104826518 title "NMR-Untersuchungen an Dialkylsubstituierten Piperidinen-I. Konfigurationsbestimmung der 2,3-, 2,4- und 3,4-Dimethylpiperidine und die Analyse Ihrer NMR-Spektren" @default.
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- W2104826518 doi "https://doi.org/10.1002/mrc.1270010105" @default.
- W2104826518 hasPublicationYear "1969" @default.
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