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- W2104927400 abstract "The structural evolution of a scandia/nitrogen co-doped zirconia sample, Sc 0.148 Zr 0.852 O 1.72 N 0.14 , was investigated by neutron powder diffraction up to 1700 °C. At ambient temperature it has an anion-deficient fluorite related β ′-type structure with ordered anion vacancies (space group R -3, a = 9.5611 Å, c = 17.5020 Å). With increasing temperature a gradual transformation into a cubic fluorite-type phase ( Fm 3 m ) with randomly distributed vacancies takes place which is accompanied by an enrichment of Sc in the rhombohedral phase and completed at ∼1050°C. At higher temperatures probability densities and single particle potentials of the anions were determined. The incorporation of nitrogen into the scandia-zirconia material significantly increased the activation energy for anion migration to values above 1 eV. The anions migrate predominantly along the <100>-directions to neighbouring sites." @default.
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- W2104927400 date "2007-07-01" @default.
- W2104927400 modified "2023-09-25" @default.
- W2104927400 title "High-temperature neutron powder diffraction study of scandia/nitrogen co-doped zirconia" @default.
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- W2104927400 doi "https://doi.org/10.1524/zkri.2007.222.7.335" @default.
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