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- W2105604562 abstract "Light green powder samples and single crystals of YbBeF 4 , YbAlF 5 , and LiYbAlF 6 have been prepared by heating appropriate mixtures of YbF 2 and BeF 2 , YbF 2 and AlF 3 , or YbF 2 , LiF, and AlF 3 at 750 °C under argon in a closed silica ampoule. YbBeF 4 crystallises monoclinic with a = 667.4(2), b = 691.1(2), c = 640.2(2) pm, β = 103.87(2)°, YbAlF 5 crystallises tetragonal with a = 1380.3(3), c = 701.3(3) pm, and LiYbAlF 6 crystallises trigonal with a = 504.2(2) and c = 986.8(1) pm. YbBeF 4 is the first fluoroberyllate, which adopts the monazite type structure, YbAlF 5 is isotypic with BaTiF 5 and LiYbAlF 6 crystallises in the LiCaAlF 6 type structure. In all three fluorides the Yb atoms are in the oxidation state +2 and the Yb-F distances range from 232 to 280 pm. Measurements of the magnetic susceptibilities have shown that YbBeF 4 , YbAlF 5 and LiYbAlF 6 are diamagnetic. The structures of YbBeF 4 , YbAlF 5 and LiYbAlF 6 are discussed in comparison to the corresponding fluoroberyllates and -fluoroaluminates with Sr and Ca." @default.
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- W2105604562 date "1999-10-01" @default.
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- W2105604562 title "Syntheses and structures of novel complex Yb(II) fluorides: YbBeF4, YbAlF5 and LiYbAlF6" @default.
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- W2105604562 doi "https://doi.org/10.1016/s1293-2558(00)80106-5" @default.
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