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- W2105656105 abstract "Naphthalene was carboxylated to naphthoic acids by the irradiation of naphthalene and a donor in the presence of carbon dioxide. The UV irradiation through Pyrex caused reactions of naphthalene, itself, giving a naphthalene dimer etc. Such undesirable reactions were partly depressed by using a CuSO4 filter solution; the selectivities of naphthoic acids and dihydronaphthalenecarboxylic acid increased from 2.2–9.8 to 12.2–23.0%. To avoid any direct irradiation to naphthalene and naphthoic acids was critical. Their high selectivities, up to 67%, were obtained upon visible light irradiation by using phenazine as a sensitizer. More than 90% of the naphthoic acids was 1-naphthoic acid, which was confirmed by GC and ms." @default.
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- W2105656105 date "2010-08-23" @default.
- W2105656105 modified "2023-09-27" @default.
- W2105656105 title "ChemInform Abstract: Photocarboxylation of Naphthalene in the Presence of Carbon Dioxide and an Electron Donor." @default.
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- W2105656105 doi "https://doi.org/10.1002/chin.199114103" @default.
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