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- W2106348447 abstract "Durch isoelektronischen Ersatz der Sauerstoffatome in SO42− durch eine CH2- und drei NtBu-Gruppen gelangt man formal zum Dianion H2CS(NtBu)32−, das nun erstmals in Form des Schwefel(VI)-Ylid-Komplexes [(tmeda)2Li2{H2CS(NtBu)3}] isoliert wurde (die Struktur ist im Bild gezeigt). Die Deprotonierung der S-gebundenen Methylgruppe im Triimidosulfonat MeS(NtBu)3− bietet einen einfachen Zugang mit hohen Ausbeuten. Bei der Hydrolyse entstehen das Triimidosulfat [{(tmeda)Li2{OS(NtBu)3]}3] und Methan und nicht, wie man auch erwarten könnte, Diimidomethylensulfat und das Amin. tmeda=Me2NCH2CH2NMe2." @default.
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- W2106348447 date "2001-10-15" @default.
- W2106348447 modified "2023-09-30" @default.
- W2106348447 title "Methylentriimidosulfat H2CS(NtBu)32− - das erste dianionische Schwefel(VI)-Ylid" @default.
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