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- W2106514245 abstract "The triblock copolymer poly(ϵ-caprolactone)-block-poly[(methyl methacrylate)-co-styrene]-block-poly(ϵ-caprolactone) was synthesized by a combination of coordination polymerization and controlled radical mechanism. The poly(ϵ-caprolactone) prepolymers (PCLBP) were first obtained by coordination polymerization using benzopinacol as the initiator and aluminium triisopropoxide as the promoter at room temperature. It was determined by means of UV and NMR spectroscopy that the benzopinacolate groups are left intact in the PCLBP prepolymers; no isomerization was found. The benzopinacolate groups incorporated into the poly(ϵ-caprolactone) then initiate the copolymerization of styrene (St) and methyl methacrylate (MMA) via a controlled radical mechanism at 95°C. The desired block copolymers were characterized by GPC, IR, UV and NMR spectroscopy in detail." @default.
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- W2106514245 date "2001-03-01" @default.
- W2106514245 modified "2023-10-14" @default.
- W2106514245 title "Synthesis and Characterization of Poly(ε-CL)-block-poly(MMA-co-St)-block-poly(ε-CL) by Combination of Coordination and Controlled Radical Polymerization" @default.
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- W2106514245 doi "https://doi.org/10.1002/1521-3927(20010301)22:5<367::aid-marc367>3.0.co;2-x" @default.
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