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- W2107503270 abstract "The number and molecular structures of the alpha-brominated 2,5-dimethylterephthalonitrile (DMT) derivatives and the dependences of the yields of derivatives on the reaction time were systematicaly investigated by means of NMR spectroscopy, MS and chromatography. The alpha-brominated DMT derivatives were comprised of 2-bromomethyl-5-methylterephthalonitrile (1), 2,5-bis(bromomethyl)terephthalonitrile (2), 2-(1,1-dibromo)methyl-5-methylterephthalonitrile (3) and 2-bromomethyl-5-(1,1-dibromo)methylterephthalonitrile (4). More than 90 % of DMT mainly transformed swiftly into 1 during the first two-hour alpha-bromination reacting, and nearly half of monobromination compound 1 converts into multibromination compounds 2, 3 and 4 in the ensuing reacting. N-bromosuccinimide (NBS) was not utterly exhausted until the reacting lasted 16 hours. The selection law in the alpha-bromination-reaction of DMT, and the close affinity between the yields of the alpha-bromination products and the reaction time were originally revealed." @default.
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- W2107503270 date "2012-02-01" @default.
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- W2107503270 title "The Molecular Structures of Alpha-Brominated 2,5-Dimethyl-Terephthalonitrile Derivatives and the Dependences of Their Yields on the Reaction Time" @default.
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- W2107503270 doi "https://doi.org/10.4028/www.scientific.net/amr.476-478.1178" @default.
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