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- W2107855862 abstract "Three supramolecular architectures, namely, (C40H44O12)·(H3O)44+·(CuCl4)24−·8H2O (1), [(C40H44O12)(CuCl2)2(H2O)4]·10H2O (2), (C40H44O12)·14H2O (3), have been successfully synthesized through the reaction of symmetrical α,α′,δ,δ′-tetramethyl-cucurbit[6]uril (TMeQ[6]) with CuCl2 at different chloride anion concentration conditions. In the structure of compound 1, which is formed in 6.0 M hydrochloric acid solution, tetrahedral [CuCl4]2− dianions and TMeQ[6] macrocycles are linked into a 1D tubular structure through hydrogen bonding, C–H⋯Cl contacts, and ion–dipole interactions. The compound 2 is isolated in 3.0 M hydrochloric acid solution, in which Cu2+ ions were found to be directly coordinated to the carbonyl oxygens of TMeQ[6] macrocycles and generated a tubular coordination polymer. A further decrease of chloride anion concentration to 1.0 M leads to compound 3, in which no Cu2+ was located and TMeQ[6] macrocycles are packed into a 3D supramolecular assembly containing numerous 1D tubular channels." @default.
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- W2107855862 date "2014-01-01" @default.
- W2107855862 modified "2023-09-23" @default.
- W2107855862 title "Anion concentration control in the self-assembly of symmetrical α,α′,δ,δ′-tetramethyl-cucurbit[6]uril-based tubular architectures" @default.
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- W2107855862 doi "https://doi.org/10.1039/c4ra01671h" @default.
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