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- W2107942773 abstract "The complex dibutyltin 2-oxo-2-phenylacetic acid 4-hydroxybenzohydrazone has been synthesized and characterized by elemental analysis, IR, 1 H and 13 C NMR, and X-ray single-crystal diffraction studies. The crystal structure belongs to triclinic, space group P-1 with <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>a</mml:mi><mml:mo>=</mml:mo><mml:mn>9.3220</mml:mn><mml:mrow><mml:mo> (</mml:mo><mml:mrow><mml:mn>10</mml:mn></mml:mrow><mml:mo>)</mml:mo></mml:mrow></mml:math> Å, <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>b</mml:mi><mml:mo>=</mml:mo><mml:mn>9.8779</mml:mn><mml:mrow><mml:mo> (</mml:mo><mml:mrow><mml:mn>11</mml:mn></mml:mrow><mml:mo>)</mml:mo></mml:mrow></mml:math> Å, <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>c</mml:mi><mml:mo>=</mml:mo><mml:mn>15.9401</mml:mn><mml:mrow><mml:mo> (</mml:mo><mml:mrow><mml:mn>17</mml:mn></mml:mrow><mml:mo>)</mml:mo></mml:mrow></mml:math> Å, <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>β</mml:mi><mml:mo>=</mml:mo><mml:mn>97.0930</mml:mn><mml:msup><mml:mrow><mml:mo> (</mml:mo><mml:mrow><mml:mn>10</mml:mn></mml:mrow><mml:mo>)</mml:mo></mml:mrow><mml:mo>∘</mml:mo></mml:msup></mml:math>, <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>Z</mml:mi><mml:mo>=</mml:mo><mml:mn>2</mml:mn></mml:math>, <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>V</mml:mi><mml:mo>=</mml:mo><mml:mn>1427.6</mml:mn><mml:mo>(</mml:mo><mml:mn>3</mml:mn><mml:mo>)</mml:mo></mml:math> Å 3 , <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mi>D</mml:mi><mml:mi>c</mml:mi><mml:mo>=</mml:mo><mml:mn>1.413</mml:mn></mml:math> mg/cm 3 , <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:mi>μ</mml:mi><mml:mo>=</mml:mo><mml:mn>0.936</mml:mn></mml:mrow></mml:math> mm −1 , <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:mi>F</mml:mi><mml:mrow><mml:mo>(</mml:mo><mml:mrow><mml:mn>000</mml:mn></mml:mrow><mml:mo>)</mml:mo></mml:mrow><mml:mo>=</mml:mo><mml:mn>628</mml:mn></mml:mrow></mml:math>, <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:mi>R</mml:mi><mml:mo>=</mml:mo><mml:mn>0.1158</mml:mn></mml:mrow></mml:math>, and <mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML><mml:mrow><mml:mi>wR</mml:mi><mml:mo>=</mml:mo><mml:mn>0.2522</mml:mn></mml:mrow></mml:math>. X-ray analysis indicates that O(2), N(2), O(4), and O(4)#1 from the ligand and O(5) from ethanol molecule are in the equatorial positions; the axial positions are occupied by two n -butyl groups. It shows a distorted pentagonal bipyramid configuration with seven-coordination for central tin atom. Fascinatingly, the supramolecular infrastructures are observed, which exist as two-dimensional sheets assembled from the organometallic subunits through intermolecular and intramolecular O–H⋯X or C–H⋯X (X = O or N) hydrogen bonds." @default.
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- W2107942773 date "2011-04-11" @default.
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- W2107942773 title "Synthesis, Characterization, and Crystal Structure of a Diorganotin(IV) Complex with 2-Oxo-2-Phenylacetic Acid 4-Hydroxybenzohydrazone" @default.
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- W2107942773 doi "https://doi.org/10.5402/2011/708162" @default.
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