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• W2108270922 startingPage "14514" @default.
• W2108270922 abstract "The new binary mixed-valence fluoride of germanium, Ge3F8, has been obtained by heating GeF4 with powdered Ge in an autoclave (390 K/4 bar/48 h). The structure contains pyramidal GeIIF3 and octahedral GeIVF6 units, linked by fluoride bridges. The new compound is the missing member of the series (GeF2)n·GeF4 (n = 2, 4, or 6). Sublimation of (GeF2)n·GeF4in vacuo provides a convenient source of GeF2 in ca. 30% overall yield." @default.
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• W2108270922 date "2014-08-14" @default.
• W2108270922 modified "2023-10-12" @default.
• W2108270922 title "The preparation and structure of Ge₃F₈– a new mixed-valence fluoride of germanium, a convenient source of GeF₂" @default.
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• W2108270922 doi "https://doi.org/10.1039/c4dt02265c" @default.
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