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- W2108332446 abstract "[120317-69-3] C4H8N3I (MW 225.03 g mol−1)InChI = 1S/C4H8N3.HI/c1-6-3-5-7(2)4-6;/h3-4H,1-2H3;1H/q+1;/p-1InChIKey = IMFBMMNQDMTHGG-UHFFFAOYSA-M(oxidation, organocatalysis)Physical Data: mp 119–123 °CForm Supplied in: crystalline white solid.Solubility: sol MeOH, THF, CH2Cl2, i-PrOH.Analysis of Reagent Purity: The compound is isolated after recrystallization (acetone) as colorless scales; mp 119–123 °C, analysis calculated for C4H8N3I: C, 21.35; H, 3.58; N, 18.67. Found: C, 21.32; H, 3.45; N, 18.45. 1H NMR (DMSO-d6) δ: 4.12 (s, 3H, N-CH3), 4.15 (s, 3H, N-CH3), 9.26 (s, 1H, C3H), 10.25 (s, 1H, C5H); 13C NMR (DMSO-d6) δ: 34.2 (q), 143.2 (d, C3), 145.1 (d, C5).Preparation: the synthesis of the azolium 1 is normally prepared by the methylation of N-methyl-1,2,4-trizaole (eq 1).1 The crude product is then recrystallized from acetone. (1)Purification: the azolium salt 1 is normally purified by recrystallization from acetone.Handling, Storage, and Precautions: no precautions concerning handling or storage have been reported." @default.
- W2108332446 created "2016-06-24" @default.
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- W2108332446 date "2011-09-15" @default.
- W2108332446 modified "2023-10-01" @default.
- W2108332446 title "1,4-Dimethyl-1H-1,2,4-triazol-4-ium Iodide" @default.
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- W2108332446 doi "https://doi.org/10.1002/047084289x.rn01389" @default.
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