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- W2108334802 abstract "The title compound (7) was synthesized in six steps from 1,8,9,10-tetrachloro-11,11-dimethoxy-endo-tricyclo[6.2.1.02,7]undeca-4,9-diene-3,6-dione (4) in an overall yield of 36%. The key intermediate, 1,8,9,10-tetrachloro-11,11-dimethoxy-endo-tricyclo-[6.2.1.02,7]undeca-3,5,9-triene (12), obtained from 4 by reduction, mesylation and then 1,4-elimination, was allowed to react with diethyl azodicarboxylate to afford the Diels-Alder adduct 16. Photochemical closure of 16, followed by hydrolysis and decarboxylation, gave the title compound. The title compound failed to give either the homopentaprismanone derivative 3 or the diene 9 by the photochemical or thermal elimination of molecular nitrogen." @default.
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- W2108334802 date "1986-09-01" @default.
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- W2108334802 title "Studies on Cage Compounds. Synthesis of 8,11-Diazenediyl-4,4-Dimethoxy-2,3,5,6-Tetrachloropentacyclo[5.4.0.0<sup>2,5</sup>.0<sup>3,10</sup>.0<sup>5,9</sup>]Undecane" @default.
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- W2108334802 doi "https://doi.org/10.1002/jccs.198600030" @default.
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