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- W2108386055 abstract "Erstmals dargestellt wurde Li6[CoO4] in Form transparenter blauer Einkristalle (Tempern inniger Gemenge von Li2O, Na2O und „CoO”︁ (Li:Na:Co = 1,3:1,3:1) in Co-Bömbchen, 580°C, 22 d), die tetragonal kristallisieren, Gemäß Li6□CoO4 liegt eine geordnete Variante des Li2O-Typs vor: R.-Gr. P42/nmc; a = 653,6(1) pm, c = 465,4(1) pm; Z = 2; drö = 2,75 g · cm−3, dpyk = 2,71 g · cm−3 (Vierkreisdiffraktometerdaten (PW 1100), AgKα; 230 von 936 I0(hkl); R = 9,58%, RW = 5,25%). Parameter siehe Text. Der Madelunganteil der Gitterenergie, MAPLE, und Effektive Koordinationszahlen, ECoN, diese über Mittlere Fiktive Ionenradien, MEFIR, werden berechnet und diskutiert. Die magnetischen Eigenschaften wurden im Temperatur-bereich 14–297 K gemessen. A New Cobaltate with Isolated Anion Structure: Li6[CoO4] For the first time transparent, blue single crystals of Li6[CoO4] have been prepared (Li2O/Na2O/„CoO”︁ (Li:Na:Co = 1.3:1.3:1), Co-tube, 580°C, 22 d). Corresponding to Li6□CoO; it is an ordered variant of the Li2O-type of structure: P42/nmc; a = 653.6(1) pm, c = 465.4(1) pm; Z = 2; dx = 2.75 g cm−3, dpyk = 2.71 g cm−3 (4-circle-diffractometer-data (PW 1100), AgKα; 230 from 936 I0(hkl); R = 9.58%, RW = 5.25%). Parameters see text. The Madelung Part of Lattice Energy, MAPLE, and Effective Coordination Numbers, ECoN, these via Mean Fictive Ionic Radii, MEFIR, are calculated and discussed. The magnetic properties are measured in the temperature range of 14–297 K." @default.
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- W2108386055 date "1986-03-01" @default.
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- W2108386055 title "Ein neues Cobaltat mit Inselstruktur: Li6[CoO4]" @default.
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- W2108386055 doi "https://doi.org/10.1002/zaac.19865340308" @default.
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