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- W2108466165 abstract "The title compound (systematic name: μ-oxo-bis{[4,15-bis(ethoxycarbonyl)-5,14-dimethyl-2,7,13,17-tetraazatricyclo[16.4.0.07,12]docosa-3,5,7,9,11,13,15,18(1),19,21-decaene-2,17-diido]iron(III)} sesquihydrate), [Fe2(C26H26N4O4)O]·1.5H2O, crystallizes in the monoclinic space group C2/c and has two iron centres which are coordinated by macrocyclic ligands with an N4 donor set. These iron centres are bridged by a μ-oxo ligand, resulting in the formation of a dinuclear complex unit. The μ-oxo ligand interacts with a water molecule via strong hydrogen bonds. These solvent molecules aggregate by additional hydrogen bonds, producing a tetranuclear aggregate. Towards the outer rim of the cavity formed by the carboxyethyl substituents attached to the tetraaza-annulene systems there are additional solvent molecules. Due to much weaker hydrogen-bond interactions, the latter are disordered and have site-occupancy factors less than 1." @default.
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- W2108466165 date "2006-02-15" @default.
- W2108466165 modified "2023-10-09" @default.
- W2108466165 title "μ-Oxo-bis[(diethyl 6,17-dimethyldibenzo[<i>a</i>,<i>h</i>]-5,9,14,18-tetraaza[14]annulene-7,16-dicarboxylato)iron(III)] sesquihydrate" @default.
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- W2108466165 doi "https://doi.org/10.1107/s1600536806004636" @default.
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