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• W2108504916 abstract "Abstract Zinc reduction of Cp* 2 W 2 O 5 in an acidified water–methanol medium affords the green 3‐electron trinuclear cluster [Cp* 3 W 3 O 4 (OH) 2 ] 2+ , isolated and crystallographically characterized as the triflate salt, 1 . Upon exposure to air, this complex is oxidized to a related 2‐electron cluster, [Cp* 3 W 3 O 6 ] + , which was crystallized and characterized in three different salts, 2 – 4 . The 3‐electron cluster exhibits a near‐tetragonal frozen‐glass EPR spectrum, and it shows evidence of coupling of the unpaired electron to only one of the three W atoms. The two‐electron cluster is diamagnetic. An electrospray ionization MS n study revealed a stepwise expulsion of neutral [Cp*WO 2 ] units as the main fragmentation process. DFT calculations unveiled the intimate details of the electronic structures of these complexes and fully rationalized the structural and spectroscopic properties.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)" @default.
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• W2108504916 date "2007-09-01" @default.
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• W2108504916 title "Aqueous Reduction of [Cp*₂W₂O₅]: Characterization of the Triangular Clusters [Cp*₃W₃O₄(OH)₂]²⁺and [Cp*₃W₃O₆]⁺– Comparison with Molybdenum" @default.
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• W2108504916 doi "https://doi.org/10.1002/ejic.200700419" @default.
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