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- W2108663015 abstract "Abstract This study examined the use of a new tetrafunctional peroxide initiator in the bulk free‐radical polymerization of methyl methacrylate. The objective was to investigate the effect of using a multifunctional initiator through an examination of the rates of polymerization and the polymer properties. The molecular weights and radii of gyration were obtained with a size exclusion chromatograph equipped with an online multi‐angle laser light scattering detector. The performance of the tetrafunctional initiator was compared to that of a monofunctional counterpart [ tert ‐butylperoxy 2‐ethylhexyl carbonate (TBEC)]. The results showed that the new tetrafunctional peroxide initiator produced a faster rate of polymerization than TBEC at an equivalent concentration but also generated a polymer of a lower molecular weight. This trend was the opposite of what was observed in a previous study with styrene. When TBEC was used at a concentration four times that of the new tetrafunctional peroxide initiator, both produced equal rates of polymerization and similar molecular weights. The degree of branching was also investigated with radius‐of‐gyration plots. © 2004 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 42: 5647–5661, 2004" @default.
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- W2108663015 date "2004-10-01" @default.
- W2108663015 modified "2023-10-13" @default.
- W2108663015 title "Free-radical polymerization of methyl methacrylate with a tetrafunctional peroxide initiator" @default.
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- W2108663015 doi "https://doi.org/10.1002/pola.20389" @default.
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