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- W2108736083 abstract "Commercially available cyanoethyl phosphoramidites derived from T, d(C), d(A), and d(G) were hydrolyzed (1H-tetrazole, MeCN/H2O) to give the corresponding H-phosphonates in excellent yields. Palladium(0)-catalyzed cross-coupling of each of these with the thymidine-derived vinylbromide 2 afforded the corresponding vinylphosphonate-linked dimers T*T, d(C)*T, d(A)*T, and d(G)*T in modest to good yields. The T*T dimer was further elaborated to give a 5‘-DMT-T*T-3‘-CEP building block, and this was used in the automated synthesis of the TpT*TpT tetramer." @default.
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- W2108736083 date "2001-09-25" @default.
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- W2108736083 title "Commercially Available 5‘-DMT Phosphoramidites as Reagents for the Synthesis of Vinylphosphonate-Linked Oligonucleic Acids" @default.
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- W2108736083 doi "https://doi.org/10.1021/ol0166045" @default.
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