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- W2108751625 abstract "Abstract The reaction of 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane-2,4-disulfide (Lawesson's Reagent) with two different Grignard reagents gave the corresponding dithiophos-phinic acids (DTPA), CH3OC6H4-(R)P(S)SH; [R = iso-butyl (HL1) and sec-butyl (HL2)]. HL1 and HL2 were treated with dry ammonia to convert them to the ammonium salts, NH4L1 and NH4L2. Ni(II) and Co(II) complexes of L1 and L2 – [Ni(L1)2], [Ni(L2)2]; [Co(L1)2]2 and [Co(L2)2]2—were obtained by the reaction of NH4L1 and NH4L2 with NiCl2.6H2O and CoCl2.6H2O, respectively, in ethanol. Square-planar nickel complexes [Ni(L1)2] and [Ni(L2)2] were further reacted with pyridine (Py) to obtain the octahedral complexes, [Ni(Py)2(L1)2] and [Ni(Py)2(L2)2]. The compounds were characterized by elemental analysis, FTIR, APCI/ESI-MS and 1H, 13C, and 31P NMR spectroscopies. The novel nickel(II) complex [Ni(L2)2] was characterized by X-ray crystallography. Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements for the following free supplemental resource: Figures S1-S5." @default.
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- W2108751625 date "2012-01-05" @default.
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- W2108751625 title "Synthesis and Spectroscopic Characterizations of Novel Ni(II) and Co(II) Dithiophosphinate Complexes, and X-Ray Studies on the Ni(II) Complex" @default.
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- W2108751625 doi "https://doi.org/10.1080/10426507.2011.601239" @default.
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