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- W2108803328 abstract "Abstract 2,2′‐Biphenol‐ and ( R / S )‐ and ( R )‐1,1′‐bi(2‐naphthol)‐based polysulfones were synthesized by classical step‐growth polymerizations and by entropically‐driven ring‐opening polymerizations (ED‐ROPs) of the corresponding macrocyclic oligomers (MCOs). To facilitate comparisons, the polysulfone derived from 4,4′‐cyclohexylidenebisphenol was synthesized similarly. ED‐ROP was also used to prepare copolymers. The molecular weights obtained using ED‐ROP were generally higher than those obtained using the classical step growth method. The MCOs required as the starting materials for ED‐ROPs were prepared by classical high dilution syntheses using the biphenols and bis(4‐chlorophenyl)sulfone in the presence of base. The cyclic dimer from a high dilution synthesis using ( R )‐1,1′‐bi‐2‐naphthol and the cyclic dimer from a similar synthesis using 4,4′‐cyclohexylidenebisphenol were isolated as pure compounds by column chromatography and the molecular structures determined by single crystal X‐ray diffraction. Copyright © 2006 John Wiley & Sons, Ltd." @default.
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- W2108803328 date "2006-08-23" @default.
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- W2108803328 title "Synthesis of 2,2′-biphenol- and 1,1′bi(2-napthol)-based poly(ether sulfones) and copolymers by classical step-growth polymerization and by entropically-driven ring-opening polymerization of macrocyclic oligomers" @default.
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- W2108803328 doi "https://doi.org/10.1002/pat.726" @default.
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