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• W2109417170 abstract "The determination of ring size can vary from simple to complex, but the process in difficult cases can be advantageously augmented by DFT calculation of NMR parameters such as the chemical shifts of (), (), and other nuclei as well as pertinent spin-spin (scalar) coupling constants, for example, those between protons (). Differentiation between 6- and 7-membered ring formation in the case of 3,4-dihydro-2 H -3-hydroxymethyl-1,4-benzoxazine and 2,3,4,5-tetrahydro-1,5-benzoxazepine-3-ol was evaluated with a view to not only affecting 6- versus 7-membered ring differentiation generally for cases on hand, but also in the case of literature reports where the assigned structures may be in doubt. Thus, the main focus was on the usually reported NMR parameters of , , and and wherein the analysis was found to be highly successful, particularly for , and thus potentially amenable for broad application." @default.
• W2109417170 created "2016-06-24" @default.
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• W2109417170 date "2012-11-14" @default.
• W2109417170 modified "2023-09-27" @default.
• W2109417170 title "Differentiation between 6- and 7-Membered Rings Based on Theoretical Calculation of NMR Parameters" @default.
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• W2109417170 doi "https://doi.org/10.5402/2012/697156" @default.
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