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• W2109463705 abstract "The synthesis of a series of aromatic 5,6-benzannelated and naphthyl-benzannelated spiroacetals related to the spiroacetal unit present in the quinonoid antibiotic γ-rubromycin is reported. The key steps include the use of Sonogashira coupling to construct an aryl acetylene that is coupled to an aryl aldehyde forming a propargyl alcohol intermediate. Hydrogenation of the resultant alkynol followed by oxidation produces a masked dihydroxyketone that upon treatment with silica-supported sodium hydrogen sulfate undergoes concomitant deprotection and cyclisation to afford the desired fused aromatic spiroacetal." @default.
• W2109463705 created "2016-06-24" @default.
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• W2109463705 date "2007-06-01" @default.
• W2109463705 modified "2023-10-14" @default.
• W2109463705 title "Synthesis of aromatic spiroacetals related to γ-rubromycin based on a 3H-spiro[1-benzofuran-2,2′-chromane] skeleton" @default.
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• W2109463705 doi "https://doi.org/10.1016/j.tet.2007.02.033" @default.
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