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- W2109492159 abstract "New thiosemicarbazone derivatives 3a-c , obtained by the condensation of 4-(2,3-dimethyl-1-phenyl-pyrazolone-5-yl-4)-thiosemicarbazide ( 1 ) with cycloalkanones 2a-c , on reaction with mercaptoacetic acid ( 4 ) yields the corresponding spiro thiazolidin-4-ones 5a-c . Compound 5 undergo intramolecular heterocyclization to the corresponding 1-(2,3-dimethyl-1-phenyl-pyrazolone-5-yl-4)-2-mercapto-1',5-cycloalkane-spiro[1,3]thiazolo[3,4-b]-1,2,4-triazoles 6a-c with NaOH. centerline{epsfbox{:art:fig-01a.jpg}}" @default.
- W2109492159 created "2016-06-24" @default.
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- W2109492159 date "2003-05-01" @default.
- W2109492159 modified "2023-09-25" @default.
- W2109492159 title "Synthesis of 1-(2,3-Dimethyl-1-phenyl-pyrazolone-5-yl-4)-2-mercapto-1′,5-cycloalkane-spiro[1,3]thiazolo[3,4-b]-1,2,4-triazole Derivatives" @default.
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- W2109492159 doi "https://doi.org/10.1080/10426500307854" @default.
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!["New thiosemicarbazone derivatives 3a-c , obtained by the condensation of 4-(2,3-dimethyl-1-phenyl-pyrazolone-5-yl-4)-thiosemicarbazide ( 1 ) with cycloalkanones 2a-c , on reaction with mercaptoacetic acid ( 4 ) yields the corresponding spiro thiazolidin-4-ones 5a-c . Compound 5 undergo intramolecular heterocyclization to the corresponding 1-(2,3-dimethyl-1-phenyl-pyrazolone-5-yl-4)-2-mercapto-1',5-cycloalkane-spiro[1,3]thiazolo[3,4-b]-1,2,4-triazoles 6a-c with NaOH. centerline{epsfbox{:art:fig-01a.jpg}}"](?object=%22New%20thiosemicarbazone%20derivatives%203a-c%20%2C%20obtained%20by%20the%20condensation%20of%204-(2%2C3-dimethyl-1-phenyl-pyrazolone-5-yl-4)-thiosemicarbazide%20(%201%20)%20with%20cycloalkanones%202a-c%20%2C%20on%20reaction%20with%20mercaptoacetic%20acid%20(%204%20)%20yields%20the%20corresponding%20spiro%20thiazolidin-4-ones%205a-c%20.%20Compound%205%20undergo%20intramolecular%20heterocyclization%20to%20the%20corresponding%201-(2%2C3-dimethyl-1-phenyl-pyrazolone-5-yl-4)-2-mercapto-1'%2C5-cycloalkane-spiro%5B1%2C3%5Dthiazolo%5B3%2C4-b%5D-1%2C2%2C4-triazoles%206a-c%20with%20NaOH.%20centerline%7Bepsfbox%7B%3Aart%3Afig-01a.jpg%7D%7D%22){kind=link}