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- W2109646364 abstract "Both anti- and syn-α-hydroxy-β-amino acids are efficiently synthesized in protected form and high enantiomeric purity from readily available anti-N-Boc-1-tert-butyldimethylsilyl-3-amino-1,2-diols. The preparation of the anti series is straightforward, and takes place by protection of the secondary hydroxyl group (1-ethoxyethyl) followed by desilylation/oxidation of the primary hydroxyl group. For the preparation of the syn isomers, the secondary alcohol is inverted at the beginning of the sequence by Mitsunobu methodology (p-nitrobenzoate). Starting from homochiral (2S,3S)-N-Boc-1-tert-butyldimethylsilyl-3-amino-3-phenylpropane-1,2-diol, the ready for coupling Taxotere® side chain has been prepared in enantiomerically pure form." @default.
- W2109646364 created "2016-06-24" @default.
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- W2109646364 date "1996-01-01" @default.
- W2109646364 modified "2023-10-16" @default.
- W2109646364 title "An enantioselective, stereodivergent approach to anti- and syn-α-hydroxy-β-amino acids from anti-3-amino-1,2-diols. Synthesis of the ready for coupling taxotere® side chain." @default.
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- W2109646364 doi "https://doi.org/10.1016/0957-4166(95)00442-4" @default.
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