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- W2109918984 abstract "A facile, versatile and reproducible sol–gel process to make microporous organosilica membranes by using 1,2-bis (triethoxysilyl) ethane (BTESE) as a precursor is reported. The influence of process parameters on sol particle size and rheology of BETSE-derived sols was investigated to produce defect-free composite membranes by a single dipping procedure and subsequent calcination. The microporous structure of a BTESE layer on mesoporous alumina supports enabled selective molecular sieving of gas molecules. Single gas permeation (SGP) experiments, performed at 200 °C, showed that a H2/CH4 permselectivity of 24 was reproducibly achieved. No SF6 gas permeance through these membranes proof the presence of a defect-free microstructure. SEM cross-section analysis showed a hybrid selective layer with a thickness dependent on the sol precursor concentration." @default.
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- W2109918984 date "2013-11-01" @default.
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- W2109918984 title "Influence of sol–gel process parameters on the micro-structure and performance of hybrid silica membranes" @default.
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- W2109918984 doi "https://doi.org/10.1016/j.memsci.2013.06.024" @default.
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