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- W2110332102 abstract "The diazomethane-derived tetramethyl esters of fumonisins can be introduced readily into mass spectrometers using flow injection analysis or liquid chromatography (LC) via a particle-beam interface to yield chemical ionization and electron-ionization spectra. The esters of fumonisins B1, B2, and B3 were well resolved on a C18 reversed-phase column when eluted with a gradient of water + methanol + acetonitrile in the presence of 0.05% trifluoroacetic acid. Enhancement of analyte transport through the particle-beam interface to afford increased ion abundances was achieved by addition of carriers. Polyfunctional amino acid carriers, such as L-glutamic acid or L-serine, effected at least 100-fold increases in sensitivity. In the LC mode, post-column addition of aqueous L-serine was the most advantageous because background interference was limited to lower masses, and because of higher solubility, and ease of cleaning." @default.
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- W2110332102 date "1993-05-01" @default.
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- W2110332102 title "Detection and characterization of fumonisin mycotoxins as their methyl esters by liquid chromatography/particle-beam mass spectrometry" @default.
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- W2110332102 doi "https://doi.org/10.1002/rcm.1290070509" @default.
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