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- W2110351558 abstract "The 5‘-amino-5‘-phosphono derivatives of cytidine, cytosine arabinoside (ara-C), and uridine have been prepared via the corresponding nucleoside aldehydes. Phosphite addition to imines derived from the nucleoside aldehydes and p-methoxybenzylamine was efficient, and use of this amine allowed cleavage of the products to the parent amino phosphonic acids. The phosphite additions proved to be diastereoselective, with the cytidine and uridine derivatives favoring the 5‘S stereochemistry and the ara-C derivative favoring the 5‘R isomer. The stereochemistry of one cytidine derivative was established by single-crystal diffraction analysis, and detailed comparisons of the 13C NMR data allowed assignments of the other amino phosphonates." @default.
- W2110351558 created "2016-06-24" @default.
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- W2110351558 date "2003-12-09" @default.
- W2110351558 modified "2023-09-28" @default.
- W2110351558 title "Synthesis of 5′-Amino-5′-phosphonate Analogues of Pyrimidine Nucleoside Monophosphates." @default.
- W2110351558 cites W2953047116 @default.
- W2110351558 doi "https://doi.org/10.1002/chin.200349199" @default.
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