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- W2110491330 abstract "Two new phases, (C4H12N2)(H3O)[(VOPO4)4(H2O)H2PO4]·3H2O (1) and (C4H12N2)[(VO)(VO2)2(H2O)(PO4)2] (2) have been synthesized hydrothermally and characterized by single crystal X-ray diffraction, thermogravimetric analysis, and magnetic susceptibility. Compound 1 has an open-framework structure and is closely related to (VO)2(PO4)2H2PO4·N2C2H10, whereas compound 2 has layered structure containing discrete trinuclear [V3O13(H2O)] corner-sharing units. In both structures the V atoms are mixed-valence, VIV and VV, with octahedral and trigonal bipyramidal geometry. Crystal data: (C4H12N2)(H3O)[(VOPO4)4(H2O)H2PO4]·3H2O 1, monoclinic, space group P2/n (No. 13), a=9.6448(7) Å, b=8.8770(7) Å, c=14.813(1) Å, β=91.936(2)°, Z=4, R1=0.0717; (C4H12N2)[(VO)(VO2)2(H2O)(PO4)2] 2, triclinic, space group P1 (No. 2); a=6.1650(5) Å, b=10.8206(9) Å, c=11.854(1) Å, α=66.598(1)°, β=76.008(2)°, γ=83.439(2)°, Z=2, R1=0.0467." @default.
- W2110491330 created "2016-06-24" @default.
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- W2110491330 date "2000-11-01" @default.
- W2110491330 modified "2023-09-24" @default.
- W2110491330 title "Hydrothermal Synthesis and Characterization of Two Mixed Valence Piperazine–Vanadium Phosphates: (C4H12N2)(H3O)[(VOPO4)4(H2O)H2PO4]·3H2O and (C4H12N2)[(VO)(VO2)2(H2O)(PO4)2]" @default.
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- W2110491330 doi "https://doi.org/10.1006/jssc.2000.8872" @default.
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