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- W2110650188 abstract "Alpha-alkoxy, amino-, and thio nitriles undergo a Ti(II)-mediated coupling with Grignard reagents to afford heterofunctionalized cyclopropylamines. A chelation effect appears to be generally responsible for the spontaneous contraction of the intermediate azatitanacycle leading to cyclopropane. By using the described reaction, 1-aminocyclopropanecarboxylic acids were prepared in four steps, in good overall yields, from the readily available benzyloxyacetonitrile." @default.
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- W2110650188 date "2002-04-27" @default.
- W2110650188 modified "2023-09-30" @default.
- W2110650188 title "Ti(II)-Mediated Conversion of α-Heterosubstituted (O, N, S) Nitriles to Functionalized Cyclopropylamines. Effect of Chelation on the Cyclopropanation Step" @default.
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- W2110650188 doi "https://doi.org/10.1021/jo025634y" @default.
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