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- W2111021572 abstract "Abstract A highly regioselective halogenation reaction of symmetrical and unsymmetrical aromatic azo compounds has been developed at room temperature or at 50 °C. In the presence of 5 mol% palladium diacetate and 0.5 equiv. of p ‐toluenesulfonic acid, a range of symmetrical aromatic azo compounds smoothly undergo monobromination with N ‐bromosuccinimide to give the corresponding unsymmetrical aromatic azo compounds in good to excellent yields with >99:1 ortho ‐selectivity. This chemistry has been successfully extended to unsymmetrical aromatic azo compounds, whose electron‐richer aryl groups prefer to be monobrominated. Moreover, replacing N ‐bromosuccinimide with N ‐iodosuccinimide in the reaction allows the synthesis of monoiodinated aromatic azo compounds with >99:1 regioselectivity." @default.
- W2111021572 created "2016-06-24" @default.
- W2111021572 creator A5017824586 @default.
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- W2111021572 date "2013-01-25" @default.
- W2111021572 modified "2023-10-18" @default.
- W2111021572 title "Palladium‐Catalyzed Regioselective Halogenation of Aromatic Azo Compounds" @default.
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- W2111021572 doi "https://doi.org/10.1002/adsc.201200902" @default.
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