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• W2111805131 abstract "[52693-56-8] C6H7BrIN (MW 299.94)InChI = 1S/C6H7BrN.HI/c1-8-5-3-2-4-6(8)7;/h2-5H,1H3;1H/q+1;/p-1InChIKey = DVAZKUDTZUIOQK-UHFFFAOYSA-M(dehydrative coupling and activation of alcohols)Preparative Methods: the title reagent (1a) as well as the chloro analog (1b) can be prepared by adding 1.2 equiv of MeI to an acetone solution of 2-bromo- or 2-chloropyridine at 0 °C. After stirring for 3 days at rt the precipitated pyridinium salt is filtered off and washed with dry ether. Further drying under vacuum results in 80–90% yield of the pyridinium salt as a colorless solid which may be used without further purification.2b,c" @default.
• W2111805131 created "2016-06-24" @default.
• W2111805131 creator A5066916712 @default.
• W2111805131 date "2001-04-15" @default.
• W2111805131 modified "2023-09-26" @default.
• W2111805131 title "2-Bromo-1-methylpyridinium Iodide" @default.
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• W2111805131 doi "https://doi.org/10.1002/047084289x.rb309" @default.
• W2111805131 hasPublicationYear "2001" @default.
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