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• W2112207598 endingPage "10071" @default.
• W2112207598 startingPage "10071" @default.
• W2112207598 abstract "The reactions of 1,2,3,4-benzenetetracarboxylic acid (H4mpda) and different silver(I) salts under hydrothermal or solvent evaporation conditions yielded four unusual coordination complexes with interesting frameworks: [Ag4(mpda)]n (1), {[Ag2.5(mpda)(bpy)2]·[Ag(bpy)]·[Ag(bpy)(H2O)]·(NO3)0.5·(H2O)9}n (2), {[Ag5(mpda)2(bpy)4]·[Ag(bpy)]·[Ag(bpy)(H2O)]·[Ag(bpy)(H2O)]·(H2O)16}n (3), {[Ag2(mpda)(H2O)]·[Ag(bpy)]·[Ag(bpy)]}n (4) (bpy = 4,4′-bipyridine). Complex 1 displays a novel (3,4,7)-connected {4.62}{4.65}{42.613.85.10} topology, in which the carboxylic groups of the mpda4− ligand adopt variable coordination modes. In 1, besides Ag–O coordination bonding, Ag⋯Ag and Ag⋯aromatic intermolecular interactions also make their appearance. In complexes 2–4, rare architectures comprising three or four isolated coordination polymers within the same crystalline structure have been obtained, respectively. In 2 and 3, neighboring layers are linked together through water tapes into a three-dimensional supramolecular architecture, which is also consolidated by π⋯π stacking, while independent infinite rod-like polymer chains fill the void space between layers. Interestingly, an anionic (H2O–NO3−)n layer, built from water tapes and nitrate anions as well as consolidated by the mpda4− ligands, has been structurally identified in compound 2. A new water tape constructed from alternating tetramers and decamers has been obtained in compound 3. In compound 4, a right-handed helical chain and two rod-like polymeric chains are interconnected through host–guest molecular recognition to generate a three-dimensional chiral supramolecular architecture. Bulk materials for 1 and 4 have second-harmonic generation activity, being approximately 0.6 and 0.4 times that of urea. The IR spectra, thermogravimetric analysis and luminescent properties of all compounds were also investigated." @default.
• W2112207598 created "2016-06-24" @default.
• W2112207598 creator A5010755869 @default.
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• W2112207598 creator A5027376949 @default.
• W2112207598 creator A5034995105 @default.
• W2112207598 creator A5038881205 @default.
• W2112207598 creator A5086998836 @default.
• W2112207598 date "2011-01-01" @default.
• W2112207598 modified "2023-09-23" @default.
• W2112207598 title "Syntheses, structures and properties of silver–organic frameworks constructed with 1,2,3,4-benzenetetracarboxylic acid" @default.
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