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- W2112333058 abstract "Abstract The ErCo 3 –D 2 system has been studied by in situ neutron powder diffraction (NPD) at 60 °C and 0–16 bar deuterium pressure. Two deuteride phases were identified, β -ErCo 3 D 1.07−1.38 and γ -ErCo 3 D 3.7−4.3 . They were structurally characterized at the compositions β -ErCo 3 D 1.37 and γ -ErCo 3 D 3.7 by high-resolution neutron and synchrotron powder diffraction. In contrast to the analogous nickel systems R Ni 3 –D 2 ( R= Er, Ho; see part I, J. Alloys and Compds. 404–406 (2005) 89–94, and part II, J. Alloys and Compds. 2005, in press), their structures preserve the symmetry of the parent alloy (PuNi 3 -type, space group R -3 m ). Deuterium occupies mainly AB 2 building blocks in the β -phase, and AB 2 and AB 5 building blocks in the γ -phase. In the AB 2 building blocks cobalt is surrounded by an average of 3.8 ( β -ErCo 3 D 1.37 ) and 4.4 D-atoms ( γ -ErCo 3 D 3.7 ) in disordered distorted octahedral configurations (point symmetry −3), in contrast to nickel that is surrounded by ∼3 ( β 1 - and β 2 - R Ni 3 D x , R =Er, Ho) and ∼4 ( γ -ErNi 3 D 3.7 ) D-atoms in disordered trigonal (pyramidal) and tetrahedral configurations, respectively (point symmetry 3). These results indicate that the D-atom distributions in this homologous series depend on the nature of the transition element rather than on geometric factors, and that directional bonding effects similar to those in non-metallic complex transition metal hydrides also prevail in metallic interstitial metal hydrides." @default.
- W2112333058 created "2016-06-24" @default.
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- W2112333058 date "2006-04-01" @default.
- W2112333058 modified "2023-10-18" @default.
- W2112333058 title "Directional metal–hydrogen bonding in interstitial hydrides. III. Structural study of ErCo3Dx (0⩽x⩽4.3)" @default.
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- W2112333058 doi "https://doi.org/10.1016/j.jssc.2006.01.001" @default.
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