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- W2113072359 abstract "( m )-Menthol reacts with phosphorus trichloride to afford menthyl phosphorodichloridite 2 , which further reacts with racemic 1,1'-binaphthalene-2,2'-diol to give phosphite ( - ) -3 in the presence of triethylamine. ( - ) -3 can be easily separated by fractional crystallization to form the crystal (+)-( S ) -3 and the mother liquor ( m )-( R ) -3 . Then both the crystal and the mother liquor are treated with the AcOH-H 2 O to obtain enantiomeric pure ( m )-( S ) -1 and (+)-( R ) -1 respectively, with enantiomeric excess up to 99.7%." @default.
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- W2113072359 date "2002-01-01" @default.
- W2113072359 modified "2023-09-24" @default.
- W2113072359 title "An Improved Method for the Resolution of 1,1′-Binaphthalene-2,2′-Diol via a Phosphite Using (−)-Menthol as a Resolving Agent" @default.
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