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• W2113155441 abstract "AuCl3-catalyzed formal [4 + 2]-cycloadditions between substituted allenes and N-hydroxyanilines are described. This reaction sequence comprises initial isomerizations of allenes to butadienes under N2 and subsequent oxidations of N-hydroxyanilines to nitrosoarenes under O2. CuCl2 (5 mol %) was added in the second step to increase the oxidation efficiency. The reactions are compatible with various 1,1-di- and 1,1,3-trisubstituted allenes and N-hydroxyaniline derivatives. Our experimental data reveal that the roles of AuCl3 are 3-fold, including catalytic oxidations of N-hydroxyaniline derivatives to nitrosoarenes, isomerizations of alkyl-substituted allenes to dienes, and final nitroso/butadiene [4 + 2] cycloadditions." @default.
• W2113155441 created "2016-06-24" @default.
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• W2113155441 date "2014-04-30" @default.
• W2113155441 modified "2023-10-08" @default.
• W2113155441 title "Catalytic Formal [4 + 2] Cycloadditions between Unactivated Allenes and <i>N</i>-Hydroxyaniline Catalyzed by AuCl₃/CuCl₂/O₂" @default.
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• W2113155441 doi "https://doi.org/10.1021/jo500009x" @default.
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